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A simplified quantitative Kreis test has been compared with peroxide numbers and iodine values during prolonged rancidification of several animal and vegetable fats. Search SpringerLink. July 1946, Volume 23, Issue 7, pp 222–225 Cite as. Comparison of a simplified, quantitative kreis test with peroxide. Qualification Visits GMP / GDP inspectors can be a serious problem, unless you have the proper equipment or adequate documentation on the control of temperature and environmental conditions. In the worst case, there is a risk of product recall, the huge financial deficit and the loss of good reputation in the pharmaceutical industry.
• 99 Downloads • Summary 1. A simplified quantitative Kreis test has been compared with peroxide numbers and iodine values during prolonged rancidification of several animal and vegetable fats. The ratio of Kreis to peroxide values varied with the kind of fat and seemed to parallel its linoleic acid content. With vegetable oils containing a large amount of linoleic acid (corn and cottonseed) the intensity of color at the time of peak color development was too great to be read on the colorimeter. With all fats for which accurate determinations were possible (butter, chicken, pork, and ethyl oleate), the Kreis values reached maximum and began falling off while peroxide values were still increasing. Temperature of fat storage had a greater effect on the Kreis test than on the peroxide number. Increasing the temperature caused a decrease not only in the peak values obtained for the Kreis test, but also in the ratio of Kreis to peroxide values.
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